T/GXAF 0011-2023 Active Group standards

T/GXAF 0011-2023 Determination of 2-Acetyl-1-Pyrrolidine in Rice Using Gas Chromatography-Mass Spectrometry (GC-MS) method

T/GXAF 0011-2023 Determination of 2-Acetyl-1-Pyrrolidine in Rice Using Gas Chromatography-Mass Spectrometry (GC-MS) method

Publish Date: 2023-04-10 Implement Date: 2023-05-01 For services related to genuine standard inquiry, procurement, translation, and other related services in China, please Contact Us
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Basic Information

Standard Code: T/GXAF 0011-2023
Standard Type: Group standards
Standard Status: Active
is_force_gb: no
CCS Name: -
ICS Name: Integrated agriculture and forestry
Publish Date: 2023-04-10
Implement Date: 2023-05-01

Scope

Main technical content: This document describes the principle of determining the content of 2-acetyl-1-pyrroline in rice by gas chromatography-mass spectrometry, and stipulates the requirements for reagents and materials, instruments and equipment, analysis steps, result calculation and expression, and precision. This document is applicable to the determination of the content of 2-acetyl-1-pyrroline in rice, with a detection limit of 0.005 mg/kg and a determination limit of 0.015 mg/kg. The principle is as follows: The rice samples are extracted with dichloromethane under water bath heating conditions, and then determined by gas chromatography-mass spectrometry, with quantification using the internal standard method.

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