T/NMRJ 019-2024 The determination of cyanide in solid waste by flow injection spectrophotometric method using p-isonitrobenzene sulfonic acid and barbituric acid
T/NMRJ 019-2024 The determination of cyanide in solid waste by flow injection spectrophotometric method using p-isonitrobenzene sulfonic acid and barbituric acid
Basic Information
Scope
Scope: This document specifies the flow injection azide-barbituric acid spectrophotometric method for the determination of cyanide in solid waste. This document is applicable to the determination of cyanide in solid waste. When the detection optical path is 10 mm, the detection limit of cyanide in solid waste by the flow injection azide-barbituric acid spectrophotometric method is 0.001 mg/L, and the determination limit is 0.004 mg/L; Main technical content: This method specifies the flow injection-spectrophotometric method for the determination of cyanide in solid waste. This standard is applicable to the determination of cyanide in solid waste. The main technical points of this method are the preparation method of the leaching solution of cyanide in solid waste. According to the "Leaching Toxicity Method for Solid Waste - Sulphuric Acid Nitric Acid Method (HJ/T 299)", the "Technical Specifications for the Identification of Hazardous Waste (HJ/T 298)" and the physicochemical properties of cyanide, the extraction medium and time conditions are determined; the working conditions of the flow injection instrument are specified.