T/CCAA 73-2023 Determination of 34 foodborne stimulants including prednisone, prednisolone, and methylprednisolone by liquid chromatography-tandem mass spectrometry

Scope

Scope: This document specifies the determination methods for prednisone, prednisolone, methylprednisolone, dexamethasone, betamethasone, beclomethasone, fluorohydrocortisone, fluorohydrocortisone acetate, hydrocortisone, methyltestosterone, stanozolol, methyltestosterone, phenylpropanolone, nandrolone, nandrolone phenylpropionate, nandrolone phenylbutyrate, boldenone, hydrochlorothiazide, acetazolamide, chlorthalidone, chlorothiazide, furosemide, bendroflumethiazide, amiloride, spironolactone, ketoconazole, torasemide, bumetanide, synephrine, quinidine, tolazamide, and adrenaline in food products. This document is applicable to pork and pork-containing foods, poultry and poultry-containing foods, aquatic products and aquatic-containing foods, eggs and egg-containing foods, milk and milk-containing foods, vegetables and fruits and vegetable-containing foods, condiments and condiment-containing foods, honey and honey-containing foods, cocoa and cocoa-containing foods, and the determination of prednisone, prednisolone, methylprednisolone, dexamethasone, betamethasone, beclomethasone, fluorohydrocortisone, fluorohydrocortisone acetate, hydrocortisone, methyltestosterone, stanozolol, methyltestosterone, phenylpropanolone, nandrolone, nandrolone phenylpropionate, nandrolone phenylbutyrate, boldenone, hydrochlorothiazide, acetazolamide, chlorthalidone, chlorothiazide, furosemide, bendroflumethiazide, amiloride, spironolactone, ketoconazole, torasemide, bumetanide, synephrine, quinidine, tolazamide, and adrenaline in food products. Main technical content: Table of Contents Ⅰ Preface Ⅱ 1 Scope 12 Normative Reference Documents 13 Terms and Definitions 14 Principles 15 Reagents and Materials 16 Instruments and Equipment 37 Analytical Steps 48 Presentation of Analytical Results 89 Precision 810 Detection and Quantification Limits 8 Appendix A 9 Appendix B

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