T/GDFCA 107-2024 High-throughput rapid determination of 14 fungal toxins in health food using ultra-high performance liquid chromatography-tandem mass spectrometry

Scope

Scope: This document describes a high-throughput rapid determination method for the content of 14 types of mycotoxins in health foods using ultra-high performance liquid chromatography-tandem mass spectrometry, including the principles of the method, reagents and materials, instruments and equipment, sample preparation, analysis steps, result calculation, sensitivity, accuracy, and precision requirements. This document is applicable to the determination of the content of 14 types of mycotoxins, including aflatoxin B1, aflatoxin B2, aflatoxin G1, aflatoxin G2, fumonisin B1, fumonisin B2, fumonisin B3, zearalenone, deoxynivalenol, T-2 toxin, ochratoxin A, penicillin X, and patulin, in oral liquids, tablets, capsules, granules, and other health foods. The determination of mycotoxins in raw materials and other plant-based foods for health foods can be carried out with reference to this document. Main technical contents: 4 Principles 5 Reagents and Materials 6 Instruments and Equipment 7 Sample Preparation 8 Determination Steps 9 Result Calculation and Presentation 10 Sensitivity and Precision

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