T/SXSL 09-2022 Determination of Residual Amounts of Nitroimidazoles and Their Metabolites in Feed by Liquid Chromatography-Tandem Mass Spectrometry
T/SXSL 09-2022 Determination of Residual Amounts of Nitroimidazoles and Their Metabolites in Feed by Liquid Chromatography-Tandem Mass Spectrometry
Basic Information
Scope
Main technical content: This document specifies the liquid chromatography-tandem mass spectrometry method for determining the content of 2-metronidazole, 4-nitroimidazole, ornidazole, benznidazole, dimetridazole, metronidazole, carbenicillin, chlorometronidazole, roxithromycin, hydroxymethylmetronidazole, hydroxy metronidazole, hydroxypropylmetronidazole, secnidazole, tinidazole, and propylthiazole in feed. This document is applicable to the determination of the content of 2-metronidazole, 4-nitroimidazole, ornidazole, benznidazole, dimetridazole, metronidazole, carbenicillin, chlorometronidazole, roxithromycin, hydroxymethylmetronidazole, hydroxy metronidazole, hydroxypropylmetronidazole, secnidazole, tinidazole, and propylthiazole in compound feed, concentrated feed, concentrate supplements, and premixed feed additives. The detection limit of 2-metronidazole, 4-nitroimidazole, ornidazole, benznidazole, dimetridazole, metronidazole, carbenicillin, chlorometronidazole, roxithromycin, hydroxymethylmetronidazole, hydroxy metronidazole, hydroxypropylmetronidazole, secnidazole, tinidazole, and propylthiazole in this document is 1.0 ug/kg, and the quantification limit is 3.0 ug/kg.