T/GDSES 2-2022 Water quality determination of antibiotics compounds using solid-phase extraction-high performance liquid chromatography-tandem mass spectrometry
T/GDSES 2-2022 Water quality determination of antibiotics compounds using solid-phase extraction-high performance liquid chromatography-tandem mass spectrometry
Basic Information
Scope
Scope: This document specifies the method for the determination of 32 antibiotic compounds in water by solid-phase extraction-high performance liquid chromatography-tandem mass spectrometry (SPE-HPLC-MS/MS). This document is applicable to the qualitative and quantitative detection of antibiotic compounds in surface water, urban wastewater treatment plant effluents, and aquaculture wastewater. After verification, the qualitative and quantitative detection of antibiotic compounds in groundwater and other types of wastewater can also refer to this document. Main technical content: Foreword 1. Scope of application 2. Normative reference documents 3. Terms and definitions 4. Methods and principles 5. Interference and elimination 6. Reagents and materials 7. Instruments and equipment 8. Samples 9. Analysis steps 10. Result calculation and presentation 11. Precision and accuracy 12. Quality assurance and quality control 13. Waste disposal Appendix A (informative) Basic information on antibiotic compounds Appendix B (normative) Method detection limit and determination limit Appendix C (informative) Reference conditions for liquid chromatography Appendix D (informative) Reference conditions for mass spectrometry Appendix E (informative) Mass spectra of standard substances and internal standards Appendix F (informative) Precision and accuracy of the method