T/GDFCA 107-2023 High-throughput rapid determination of 14 mycotoxins in dietary supplements using ultra-high performance liquid chromatography-tandem mass spectrometry
T/GDFCA 107-2023 High-throughput rapid determination of 14 mycotoxins in dietary supplements using ultra-high performance liquid chromatography-tandem mass spectrometry
Basic Information
Scope
Scope: This document describes a high-throughput rapid determination method for the content of 14 kinds of mycotoxins in health foods using ultra-high performance liquid chromatography-tandem mass spectrometry (UPLC-MS/MS). This document is applicable to the determination of the content of 14 mycotoxins, including aflatoxin B1, aflatoxin B2, aflatoxin G1, aflatoxin G2, ochratoxin A, ochratoxin B1, ochratoxin B3, zearalenone, deoxynivalenol, T-2 toxin, ochratoxin A, citrinin, and patulin, in health foods such as oral liquids, tablets, capsules, and granules. The determination of these mycotoxins in raw materials and other plant-based foods of health foods can be carried out as a reference. Main technical contents: 4. Principle 5. Reagents and materials 6. Instruments and equipment 7. Sample preparation 8. Determination steps 9. Result calculation and expression 10. Sensitivity and precision