T/GDSES 3-2022 Soil determination of antibiotics using ultrasonic extraction-solid phase extraction-high performance liquid chromatography-tandem mass spectrometry
T/GDSES 3-2022 Soil determination of antibiotics using ultrasonic extraction-solid phase extraction-high performance liquid chromatography-tandem mass spectrometry
Basic Information
Scope
Scope: This document specifies the ultrasonic extraction-solid phase extraction-high performance liquid chromatography-tandem mass spectrometry method for the determination of 17 antibiotic compounds in soil. This document is applicable to the qualitative and quantitative detection of antibiotic compounds in soil. After verification, the qualitative and quantitative detection of antibiotic compounds in sediments can also refer to this document. Main technical content: Foreword 1 Scope 2 Normative reference documents 3 Terms and definitions 4 Methods and principles 5 Interference and elimination 6 Reagents and materials 7 Instruments and equipment 8 Samples 9 Analysis steps 10 Result calculation and presentation 11 Precision and accuracy 12 Quality assurance and quality control 13 Waste disposal Appendix A (Normative) Basic information on antibiotic compounds Appendix B (Normative) Method detection limit and determination limit Appendix C (Informative) Liquid chromatography reference conditions Appendix D (Informative) Mass spectrometry reference conditions Appendix E (Informative) Spectra of standard substances and extraction internal standard substances Appendix F (Informative) Precision and accuracy of the method