T/GZNFS 001.4-2019 Chemical Analysis Methods for Tungsten Slag - Part 4: Determination of Phosphorus Content
T/GZNFS 001.4-2019
Basic Information
Scope
Scope: This part of T/GZNFS 001 specifies the method for determining the phosphorus content in alkali slag (tungsten slag) produced during the alkali decomposition process of ammonium paratungstate. This part is applicable to the determination of phosphorus content in alkali slag (tungsten slag) produced during the alkali decomposition process of ammonium paratungstate. The determination range (mass fraction) is 0.10% to 10.00%; Main technical content: After the sample is alkali-melted and extracted, phosphorus is coprecipitated with beryllium hydroxide as a carrier in an ammonia solution to separate it from other elements. In a nitric acid solution with a certain acidity, ammonium vanadate-ammonium molybdate is used as a color reagent, and its absorbance is measured at 420 nm using a spectrophotometer.