GB/T 14455.7-2008
Active
National standards
GB/T 14455.7-2008 Fragrance/Flavor substances—Determination of ester value after acetylation and evaluation of free alcohols and total alcohols content
GB/T 14455.7-2008 Fragrance/Flavor substances—Determination of ester value after acetylation and evaluation of free alcohols and total alcohols content
Basic Information
Standard Code:
GB/T 14455.7-2008
Standard Type:
National standards
Standard Status:
Active
is_force_gb:
no
CCS Name:
Perfume and fragrances
ICS Name:
Essential oil
Publish Date:
2008-07-15
Implement Date:
2008-11-01
Pages:
9 pages
Scope
The first method of GB/T 14455 specifies a method for evaluating the content of free alcohols and total alcohols in essential oils and determining the alcohol content of single-separated and synthetic fragrances by measuring the ester value before and after acetylation of the sample with acetic anhydride in the presence of sodium acetate. This method is not suitable for essential oils containing a large amount of tertiary alcohols (such as linalool and pinene alcohol), as tertiary alcohols cannot be completely acetylated; nor is it suitable for essential oils containing a large amount of phenols, lactones, aldehydes, and ketones that are easily enolized, as these components will also be acetylated in addition to free alcohols.
Development Information
Same series standard
GB/T 14455.1-2008 Essential oils—Principles of nomenclature
GB/T 14455.3-2008 Fragrance/Flavor substances—Evaluation of solubility(miscibility) in ethanol
GB/T 14455.5-2008 Fragrance/Flavor substances—Determination of acid value or acid content
GB/T 14455.6-2008 Fragrance/Flavor substances—Determination of ester value or ester content
Replace the following standards
GB/T 14455.7-1993 Essential oils—Determination of ester value after acetylation and evaluation of free alcohols and total alcohols content
GB/T 14455.8-1993 Essential oils(containing tertiary alcohols)—Estimation of free alcohols content by determination of ester value after acetylation
GB/T 14457.6-1993 Isolate and synthetic aroma chemicals—Determination or primary or secondary alcohols content by acetylation
GB/T 14457.8-1993 Isolate and synthetic aroma chemicals—Determination of tertiary content by acetyl chloride-dimethyl aniline method
Referenced Standards
GB/T 14454.1-1993 Aromatics—Preparation of test sample
GB/T 14454.1-2008 Fragrance/Flavor substances—Preparation of test samples
GB/T 14454.14-1993 Aromatics—Preparation of standard solution, test solution and indicator solution
GB/T 14454.14-2008 Fragrance/Flavor substances—Preparation of standard solution,test solution and indicator solution
GB/T 14455.6-1993 Essential oils—Determination of ester value
GB/T 14455.6-2008 Fragrance/Flavor substances—Determination of ester value or ester content
Adopt standards
ISO 1241:1996
ISO 3794:1976
Related Standards
GB/T 11424-1989
Replaced
GB/T 11425-1989
Replaced
GB/T 11425-1989 Oil of cassia (Cinnamomum cassia nees)
GB/T 11538-1989
Replaced
GB/T 11538-1989 Essential oils—Analysis by gas chromatography on capillary columns—General method
GB/T 11539-1989
Replaced
GB/T 11539-1989 Isolate and synthetic aromatics—Analysis by gas chromatography on packed columns—General method
GB/T 11540-1989
Replaced
GB/T 11540-1989 Isolate and synthetic aroma chemicals—Determination of relative density
GB/T 14454.11-1993
Replaced