T/CAIA SH001-2014 Active Group standards

T/CAIA SH001-2014 Monosodium glutamate sulfur compound determination using methylene blue spectrophotometry

T/CAIA SH001-2014 Monosodium glutamate sulfur compound determination using methylene blue spectrophotometry

Publish Date: 2014-12-24 Implement Date: 2015-05-01 For services related to genuine standard inquiry, procurement, translation, and other related services in China, please Contact Us
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Basic Information

Standard Code: T/CAIA SH001-2014
Standard Type: Group standards
Standard Status: Active
is_force_gb: no
CCS Name: Analysis methods for toxic substances in water environments
ICS Name: General methods for food testing and analysis
Publish Date: 2014-12-24
Implement Date: 2015-05-01

Scope

Scope: This standard specifies the method for determining the content of sulfides using the spectrophotometric method with methylene blue. This standard is applicable to the determination of sulfides (calculated as S2) in MSG ranging from 0.3 mg/kg to 4.6 mg/kg; Main technical content: The sample is dissolved in water, acidified to convert the sulfides into hydrogen sulfide, and the hydrogen sulfide is carried into an absorption solution containing triethanolamine-EDTA-sodium hydroxide by air. Under the presence of Fe(III), it reacts with N,N-dimethyl-p-phenylenediamine to form a methylene blue complex. The absorbance is measured at a wavelength of 665 nm on a spectrophotometer. The mass fraction of sulfides is calculated.

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